Region

应用

Extraction of Cimetidine on Strata™ X

样品制备详细信息

Part Number :8B-S100-TAK
Description :Strata-X 33 µm Polymeric Reversed Phase, 30 mg / 1 mL, Tubes, 100/Pk
Condition 1 :1.0 ml Methanol
Condition 2 :1.0 ml Water
Load :Load 1.00 mL Sample diluted in Buffer
Wash 1 :1.0 ml 5% methanol/D. I. water
Dry :1min at 10'' of Hg pressure
Elution 1 :1.0 ml Methanol
Evaporate: :Evaporate to dryness
Reconstitute :2 mL Mobile Phase
Notes :Blow down to almost dryness under slow stream of N2. Reconstitute with mobile phase to 200 µL. Inject 50 µL on HPLC

应用详细信息 (应用ID: 14453)

货号:00F-4249-E0
尺寸:150 x 4.6 mm ID
洗脱类型:Isocratic
洗脱A:20mM KH2PO4 (pH 7.0)
洗脱B:Methanol
梯度程序:
步骤序号 时间 (分) 图片A 图片B
1 0 90 10

流速 (毫升/分钟):1 mL/min
冷却温度: 室温
检测: UV-Vis Abs.-Fixed Wave. (UV) @ 220 nm (22°C)
备注:SecurityGuard™ Guard Cartridge System extends column lifetime.
- SecurityGuard Cartridges, C8 4 x 3.0mm, 10/Pk Part No.: AJ0-4290
- Holder Part No.: KJ0-4282

分析物详细信息

分析物详细信息不可用

1
Sulfanilimide
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2
Cimetidine
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