Region

应用

MercuryMS - Luna 3µm C18(2) 20 x 2.0mm for Benzodiazepines in Plasma by LC/MS/MS

样品制备详细信息

Part Number :8B-S100-TAK
Description :Strata-X 33 µm Polymeric Reversed Phase, 30 mg / 1 mL, Tubes, 100/Pk
Condition 1 :1 mL Methanol at 1 mL/min
Condition 2 :1 mL Water at 1 mL/min
Load :Load 1.00 mL Sample
Wash 1 :1 mL Water at 1.5 mL/min
Wash 2 :1 mL 20% MeOH in water at 1.5 mL/min
Elution 1 :1 mL Methanol at 0.5 mL/min
Evaporate: :Evaporate to dryness
Reconstitute :200 µL 15% CH3CN in water

应用详细信息 (应用ID: 16040)

尺寸:20 x 2 mm ID
洗脱类型:Gradient
洗脱A:0.1% Formic Acid in Water
洗脱B:0.1% Formic Acid in Acetonitrile
梯度程序:
步骤序号 时间 (分) 图片A 图片B
1 0 85 15
2 1 5 95
3 1.01 85 15
4 2 85 15

流速 (毫升/分钟):0.6 mL/min
冷却温度: 室温
检测: Mass Spectrometer (MS) @ amu (22°C)
备注:SecurityGuard™ Guard Cartridge System extends column lifetime.
- SecurityGuard Cartridges, C8 4 x 2.0mm, 10/Pk Part No.: AJ0-4289
- Holder Part No.: KJ0-4282

分析物详细信息

分析物详细信息不可用

1
7-Aminoflunitrazepam
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2
Chlordiazepoxide
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3
Oxazepam
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4
Nordazepam
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5
Clonazepam
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6
Temazepam
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7
Flunitrazepam
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8
Diazepam
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