Region

应用

Amphetamines in Urine by LC/MS/MS on Gemini 5µm C18 150 x 3.0

样品制备详细信息

Part Number :8B-S029-TAK
Description :Strata-X-C 33 µm Polymeric Strong Cation, 30 mg / 1 mL, Tubes, 100/Pk
Condition 1 :1 mL Methanol
Condition 2 :1 mL Water
Load :Load Sample
Wash 1 :1 mL Water
Wash 2 :1 mL 0.1M Acetic Acid
Wash 3 :1 mL Methanol
Elution 1 :1 mL 2% of ammonium hydroxide (28-30%) in methanol
Evaporate: :Evaporate to dryness
Reconstitute :200 µL Mobile Phase
Notes :to prevent the loss of amphetamine and methamphetamine during solvent evaporation, add two drops of conc. HCl before the evaporation step

应用详细信息 (应用ID: 17900)

货号:00F-4435-Y0
尺寸:150 x 3 mm ID
洗脱类型:Isocratic
洗脱A:10mM Ammonium formate w/0.1% formic acid
洗脱B:Acetonitrile
梯度程序:
步骤序号 时间 (分) 图片A 图片B
1 0 90 10

流速 (毫升/分钟):0.6 mL/min
冷却温度: 室温
检测: Mass Spectrometer (MS) @ amu (450°C)
检测器信息: SCIEX API 3000™ LC/MS/MS ESI TurboIonSpray®
heater gas flow 8000cc/min
Heater temperature 450 °C; Positive Ion Mode
备注:SecurityGuard™ Guard Cartridge System extends column lifetime.
- SecurityGuard Cartridges, Gemini C18 4 x 2.0mm, 10/Pk Part No.: AJ0-7596
- Holder Part No.: KJ0-4282

分析物详细信息

分析物详细信息不可用

1
4-Hydroxy-3-methoxymethamphetmine
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2
Amphetamine
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3
Methamphetamine
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4
3,4-Methylenedioxyamphetamine (MDA)-d5

5
3,4-Methylenedioxyamphetamine (MDA)
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6
3,4-Methylendioxymethamphetamine-d5 (MDMA)-d5

7
3,4-Methylendioxmethamphetamine (MDMA)
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