Region

应用

Simultaneous Extraction of Melamine and Cyanuric acid from Strata Melamine on Luna HILIC

样品制备详细信息

Part Number :8B-S049-FBJ
Description :Strata Melamine (55 µm, 80 Å), 200 mg / 3 mL, Tubes, 50/Pk
Condition 1 :3 mL Methanol at 1.0 mL/min
Condition 2 :3 mL Acetonitrile:Water (50/50) at 1.0 mL/min
Load :Load 3.50 mL Sample diluted in Acetonitrile:Water
Wash 1 :0.5 mL Acetonitrile:Water (50/50); 2 aliquots of at 1.0 mL/min
Wash 2 :0.5 mL Methanol:Water (50/50); 1 aliquot of at 1.0 mL/min
Wash 3 :2 at 1.0
Dry :2 mins at 10" of Hg
Elution 1 :0.5 mL Methanol at 1.0 mL/min
Elution 2 :0.5 mL 5% Ammonium Hydroxide in Methanol; 2 aliquots of at 1.0 mL/min
Evaporate: :Evaporate to dryness
Reconstitute :1 mL 90/10 : ACN/100mM ammonium formate, pH 3.2

应用详细信息 (应用ID: 18287)

货号:00D-4449-B0
尺寸:100 x 2 mm ID
洗脱类型:Isocratic
洗脱A:90/10 ACN/100 mM Ammonium Formate, pH 3.2
梯度程序:
步骤序号 时间 (分) 图片A
1 3.5 100

流速 (毫升/分钟):0.4 mL/min
冷却温度: 室温
检测: Mass Spectrometer (MS) @ (22°C)
检测器信息: * MS in -ve ionization till 1.7 mins then to +ve till 3.5 mins
备注:SecurityGuard™ Guard Cartridge System extends column lifetime.
- SecurityGuard Cartridges, HILIC 4 x 2.0mm, 10/Pk Part No.: AJ0-8328
- Holder Part No.: KJ0-4282

分析物详细信息

分析物详细信息不可用

1
Cyanuric acid
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2
Melamine
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