Region

应用

Methadone from urine by Strata-XC on a ZB-Drug1

样品制备详细信息

Condition 1 :1 mL Methanol at 1 mL/min
Condition 2 :1 mL Water at 1 mL/min
Condition 3 :2 at 1
Load :Load 1.00 mL Sample diluted in Urine
Wash 1 :1 mL 0.1 N HCl at 1 mL/min
Wash 2 :1 mL Methanol at 1 mL/min
Wash 3 :3 at 1
Dry :5 minutes at > 10 inch Hg
Elution 1 : 5% Ammonium hydroxide in methanol
Evaporate: :Evaporate to dryness
Reconstitute :50 µL Ethyl acetate

应用详细信息 (应用ID: 18485)

货号:7CD-G023-08
固定相:Proprietary Drug Phase
尺寸:10 meters x 0.18 mm x 0.18 µm
升温程序:180 °C to 340 °C @ 25 °C/min for 3.6 min
载气:Constant Flow Helium, 55 cm/sec
进样:Split 10:1 1 µL @ 280°C
检测: Mass Selective (MSD) (320°C)
备注:Methadone/Methadone-d9 is 300/600ng/mL respectively in urine
Sim ions:
(Quant ion*) D9-Methadone (*78,303): Methadone (*72,294,223)

分析物详细信息

分析物详细信息不可用

1
Methadone-d9
search

2
Methadone
search