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应用

Atenolol-Related Substance (European Pharmacopoeia) on Kinetex 2.6µm C18 150 x 4.6mm ID

应用详细信息 (应用ID: 18516)

货号:00F-4462-E0
尺寸:150 x 4.6 mm ID
洗脱类型:Isocratic
洗脱A:12.5 mM KH2PO4 in Water, pH 3.0 + 2.0g Sodium Octanesulfonate + 0.8g Tetrabutyl Ammonium Hydrogen Sulfate
洗脱B:Methanol
洗脱C:THF
梯度程序:
步骤序号 时间 (分) 图片A 图片B 图片C
1 0 80 18 2

流速 (毫升/分钟):0.6 mL/min
冷却温度: 室温
检测: UV-Vis Abs.-Variable Wave.(UV) @ 226 nm (22°C)
备注:Atenolol mobile phase was prepared as follows:
2.0 g of sodium octanesulphonate + 0.8 g of tetrabutylammonium hydrogen sulphate in 2 L of 360ml methanol + 40 mL of THF + 1600 mL of 3.4 g of potassium dihydrogen phosphate in 2 L of water (pH adjusted to 3.0- phosphoric acid)

分析物详细信息

分析物详细信息不可用

1
Impurity B

2
Impurity A

3
Impurity J
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4
Impurity I
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5
Impurity D and E

6
Impurity F

7
Impurity G

8
Impurity H