Region

应用

Extraction of Sulfa drugs using Strata X-C on Kinetex 2.6µm C18 50 x 2.1mm ID by LCMS

样品制备详细信息

Part Number :8B-S029-TBJ
Description :Strata-X-C 33 µm Polymeric Strong Cation, 30 mg / 3 mL, Tubes, 50/Pk
Condition 1 :1 mL Methanol at 2 mL/min
Condition 2 :1 mL Water at 2 mL/min
Load :Load 0.50 mL Sample diluted in 0.5
Wash 1 :1 mL 0.1M acetic acid at 2 mL/min
Wash 2 :1 mL 25% methanol/0.1M acetic acid at 2 mL/min
Wash 3 :1 at 2
Dry :2 min at 10"Hg
Elution 1 :0.5 mL 5% ammonium hydroxide/methanol at 1 mL/min
Elution 2 :0.5 mL 5% ammonium hydroxide/methanol at 1 mL/min
Evaporate: :Evaporate to dryness
Reconstitute :200 µL Initial LC mobile phase (95/5)

应用详细信息 (应用ID: 18643)

货号:00B-4462-AN
尺寸:50 x 2.1 mm ID
洗脱类型:Gradient
洗脱A:0.1% Formic acid in H2O
洗脱B:0.1% Formic acid in ACN
梯度程序:
步骤序号 时间 (分) 图片A 图片B
1 0 95 5
2 0.24 95 5
3 3.02 5 95
4 3.3 5 95
5 3.31 95 5
6 4.97 95 5

流速 (毫升/分钟):450 µL/min
冷却温度: 25 °C
检测: Mass Spectrometer (MS) @ amu (22°C)
备注:SecurityGuard™ ULTRA Guard Cartridge System extends column lifetime.
- SecurityGuard ULTRA Cartridges, UHPLC C18 for 2.1mm ID Columns, 3/Pk Part No.: AJ0-8782
- Holder Part No.: AJ0-9000

分析物详细信息

分析物详细信息不可用

1
Sulfadiazine
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2
Sulfathiazole
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3
Sulfamerazine
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4
Sulfamethoxazole
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5
Sulfaquinoxaline
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