Region

应用

Mycotoxins on Kinetex 2.6µm C18 50 x 2.1mm ID by LCMS in ESI Positive Mode (1)

样品制备详细信息

Part Number :8B-S016-EBJ
Description :Strata Screen-C (55 µm, 70 Å), 100 mg / 3 mL, Tubes, 50/Pk
Condition 1 :3 mL Methanol at 1 mL/min
Condition 2 :3 mL Water at 1 mL/min
Condition 3 :1 mL 100 mM phosphate buffer, pH 6 (adjust with phosphoric acid) at 1 mL/min
Load :Load 2.00 mL Sample diluted in 100 mm acetate buffer
Wash 1 :2 mL Water at 1 mL/min
Wash 2 :2 mL 20% acetonitrile/100 mm phosphate buffer, pH 6 at 1 mL/min
Dry :2-3 mins at 10" of Hg
Elution 1 :2 mL Ethylacetate at 1 mL/min
Elution 2 :2 mL Ethylacetate at 1 mL/min
Evaporate: :Evaporate to dryness
Reconstitute :1 mL Initial mob phase(A/B=65/35)

应用详细信息 (应用ID: 18878)

货号:00B-4462-AN
尺寸:50 x 2.1 mm ID
洗脱类型:Gradient
洗脱A:0.1% Formic acid
洗脱B:0.1% Formic acid in Acetonitrile
梯度程序:
步骤序号 时间 (分) 图片A 图片B
1 0 70 30
2 3 5 95
3 4 5 95
4 4.01 70 30
5 6 70 30

流速 (毫升/分钟):400 µL/min
冷却温度: 25 °C
检测: Mass Spectrometer (MS) @ amu (22°C)
检测器信息: ESI conditions
Positive Ionization
NEB: 12.00
CUR: 11.00
IS: 4500.00
TEM: 450.00
CAD: 11.00
EP 10.00
备注:SecurityGuard™ ULTRA Guard Cartridge System extends column lifetime.
- SecurityGuard ULTRA Cartridges, UHPLC C18 for 2.1mm ID Columns, 3/Pk Part No.: AJ0-8782
- Holder Part No.: AJ0-9000

分析物详细信息

分析物详细信息不可用

1
Fumonisin B1
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2
HT-2
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3
T2-Toxin
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4
Fumonisin B2
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5
Ochratoxin
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