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应用

Simvastatin by HPLC-Kinetex 2.6um XB-C18 150x4.6mm

应用详细信息 (应用ID: 19519)

货号:00F-4496-E0
尺寸:150 x 4.6 mm ID
洗脱类型:Isocratic
洗脱A:65:35 ACN:28mM sodium phosphate pH 4.5
梯度程序:
步骤序号 时间 (分) 图片A
1 15 100

流速 (毫升/分钟):1.5 mL/min
冷却温度: 45 °C
检测: UV-Vis Abs.-Diode Array (PDA) @ 238 nm (22°C)
备注:For USP's system suitability requirements, the capacity factor for simvastatin must not be less than 3.0; column efficiency not less than 4500 theoretical plates; tailing factor not more than 2.0; resolution, while not specified according to USP standards, should be adequate at no less than 2.0. On the Kinetex 2.6um XB-C18 150x4.6mm, the capacity factor for simvastatin is 3.0; column efficiency is 28,439; tailing factor is 1.02; and resolution between lovastatin and simvastatin is 12.57.

分析物详细信息

分析物详细信息不可用

1
Lovastatin
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2
Simvastatin
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