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应用

Ibuprofen by HPLC on Kinetex 2.6um XB-C18 100x4.6mm

应用详细信息 (应用ID: 19613)

货号:00D-4496-E0
尺寸:100 x 4.6 mm ID
洗脱类型:Isocratic
洗脱A:600:400 ACN:Water with 4g chloroacetic acid adjusted to pH 3.0 with ammonium hydroxide
梯度程序:
步骤序号 时间 (分) 图片A
1 10 100

流速 (毫升/分钟):2 mL/min
冷却温度: 30 °C
检测: UV-Vis Abs.-Variable Wave.(UV) @ 254 nm (22°C)
备注:The USP Resolution requirement between any two peaks is not less than 2.5, and the tailing factor for any individual peak is not more than 2.5. On the Kinetex 2.6um XB-C18, the resolution between Ibuprofen and Valerophenone is 5.61; valerophenone and Ibuprofen related compound C is 5.90. The tailing factors for Ibuprofen, Valerophenone and Ibuprofen related compound C are 1.61, 1.35, and 1.16, respectively. The max back pressure was 362 bar.

Compared to the LUNA 5um C18(2) 250x4.6, the run time was shorted by 4.0 min on the Kinetex 2.6um XB-C18 100x4.6mm as opposed to 2.5 min for a standard 100x4.6 column.

分析物详细信息

分析物详细信息不可用

1
Ibuprofen
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2
Valerophenone
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3
Ibuprofen related compound C