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应用

Fluoroquinolones by LCMS using Kinetex C8 2.6µm, 50 x 2.1 mm

样品制备详细信息

Part Number :8B-S100-FCH
Description :Strata-X 33 µm Polymeric Reversed Phase, 200 mg / 6 mL, Tubes, 30/Pk
Condition 1 :3 mL Methanol at 2 mL/min
Condition 2 :3 mL Water at 2 mL/min
Load :Load 10.00 mL Sample diluted in Phosphate buffer with 2% TCA
Wash 1 :2 at 2
Dry :5min @ >10 in Hg
Elution 1 :2 mL Methanol/ACN/Acetic acid 49/49/2 at 1 mL/min
Evaporate: :Evaporate to dryness
Reconstitute :500 µL 0.1% Formic acid

应用详细信息 (应用ID: 19655)

货号:00B-4497-AN
尺寸:50 x 2.1 mm ID
洗脱类型:Gradient
洗脱A:0.1% Formic acid
洗脱B:Methanol
梯度程序:
步骤序号 时间 (分) 图片A 图片B
1 0 85 15
2 5 10 90
3 6 10 90
4 6 10 90

流速 (毫升/分钟):0.4 mL/min
冷却温度: 40 °C
检测: Mass Spectrometer (MS) @ amu (550°C)
检测器信息: SCIEX API 4000™
备注:Source temp: 550ºC
Polarity: Postive
Dwell: 25 msec

分析物详细信息

分析物详细信息不可用

1
Ofloxacin
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2
Norfloxacin
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3
Norfloxacin-d5
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4
Ciprofloxacin
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5
Ciprofloxacin-d8
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6
Enrofloxacin
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7
Difloxacin
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8
Sparfloxacin
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