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应用

Humic Acids using Kinetex C8 50x2.1 mm on ABI LC-MS 4000

样品制备详细信息

Part Number :8B-S130-7CH
Description :Strata PAH, 1.5 g / 6 mL, Tubes, 30/Pk
Condition 1 :10 mL Dichloromethane at 5 mL/min
Condition 2 :20 mL Methanol at 5 mL/min
Condition 3 :20 mL MilliQ Water at 5 mL/min
Load :Load 100.00 mL Sample diluted in 75:25 MilliQ Water:Acetonitrile
Wash 1 :5 mL 50:50 Methanol:MilliQ Water at 2 mL/min
Dry :15 seconds
Elution 1 :6 mL Dichloromethane at 2 mL/min
Evaporate: :Evaporate to dryness
Reconstitute :100 µL Dichlromethane

应用详细信息 (应用ID: 19662)

货号:00B-4497-AN
尺寸:50 x 2.1 mm ID
洗脱类型:Gradient
洗脱A:5mM Ammoniium Acetate
洗脱B:Methanol
梯度程序:
步骤序号 时间 (分) 图片A 图片B
1 0 85 15
2 2 5 95
3 6 5 95
4 6.01 85 15

流速 (毫升/分钟):0.4 mL/min
冷却温度: 室温
检测: Mass Spectrometer (MS) @ 580.4 amu (22°C)
检测器信息: SCIEX API 4000™
备注:SecurityGuard™ ULTRA Guard Cartridge System extends column lifetime.
- SecurityGuard ULTRA Cartridges, UHPLC C8 for 2.1mm ID Columns, 3/Pk Part No.: AJ0-8784
- Holder Part No.: AJ0-9000

分析物详细信息

分析物详细信息不可用

1
Humic acids
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