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应用

Simvastatin by HPLC - Kinetex 2.6um C8 50x4.6mm

应用详细信息 (应用ID: 19664)

货号:00B-4497-E0
尺寸:50 x 4.6 mm ID
洗脱类型:Isocratic
洗脱A:65:35 ACN: 28mM Monobasic Sodium phosphate pH 4.5
梯度程序:
步骤序号 时间 (分) 图片A
1 15 100

流速 (毫升/分钟):1.5 mL/min
冷却温度: 45 °C
检测: UV-Vis Abs.-Diode Array (PDA) @ 238 nm (22°C)
备注:For USP's system suitability requirements, the capacity factor for simvastatin must not be less than 3.0; column efficiency not less than 4500 theoretical plates; tailing factor not more than 2.0; resolution, while not specified according to USP standards, should be adequate at no less than 2.0. While the Kinetex 2.6um C8 50x4.6 does not meet the system suitability requirement for the capacity factor for simvastatin; the capacity factor is 1.4; it does have a column efficiency of 6,984; tailing factor of 1.12; and the resolution between lovastatin and simvastatin is 4.16.

分析物详细信息

分析物详细信息不可用

1
Lovastatin
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2
Simvastatin
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