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应用

Gabapentin extracted from plasma (25 µg/mL) using PPT on a Kinetex C18 2.6µm, 50x2.1mm

应用详细信息 (应用ID: 19689)

货号:00B-4462-AN
尺寸:50 x 2.1 mm ID
洗脱类型:Gradient
洗脱A:5 mM Ammonium formate
洗脱B:Acetonitrile
梯度程序:
步骤序号 时间 (分) 图片A 图片B
1 0 97 3
2 1 97 3
3 3 10 90

流速 (毫升/分钟):0.4 mL/min
冷却温度: 室温
检测: Mass Spectrometer (MS) @ amu (22°C)
检测器信息: SCIEX API 3000™
备注:Sample prep: Combine 100µL of plasma and 100µL of 10% TCA (containing internal standard at appropriate concentration) in a centrifuge vial. Mix briefly. Centrifuge samples at 14K RPM and then transfer 100µL of supernatant to an autosampler vial. Dilute sample 10X with water before injection.

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Gabapentin-d4
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Gabapentin
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