Region

应用

Benzodiazepines from urine using Strata-X-Drug N on a Kinetex C18 2.6µm, 50x2.1mm

样品制备详细信息

Part Number :8B-S129-ECH
Description :Strata-X-Drug N 100u Polymer RP, 100mg/6mL, 30/Pk
Load :Load Sample
Wash 1 : 2 mLs of Acetonitrile:Water (20:80) (v:v)
Dry :10 minutes @ full vacuum
Elution 1 : 2mLs of Ethyl acetate:Isopropanol (85:15) (v:v)
Evaporate: :Evaporate to dryness
Reconstitute :1 mL 35% methanol in water
Notes :Evaporate eluant under a stream of N2 gas at 50ºC. Reconstitute with 1mL of 35% methanol

应用详细信息 (应用ID: 19714)

货号:00B-4462-AN
尺寸:50 x 2.1 mm ID
洗脱类型:Gradient
洗脱A:0.1% Formic acid
洗脱B:0.1% Formic acid in methanol
梯度程序:
步骤序号 时间 (分) 图片A 图片B
1 0 65 35
2 4 5 95
3 4.01 65 35
4 7 65 35

流速 (毫升/分钟):300 µL/min
冷却温度: 室温
检测: Mass Spectrometer (MS) @ amu (22°C)
检测器信息: SCIEX API 3000™

Source: Cur-11, CAD-12, IS-4500, Tem-450, NEB-12
Dwell: 25ms
Polarity: Positive
备注:SecurityGuard™ ULTRA Guard Cartridge System extends column lifetime.
- SecurityGuard ULTRA Cartridges, UHPLC C18 for 2.1mm ID Columns, 3/Pk Part No.: AJ0-8782
- Holder Part No.: AJ0-9000

分析物详细信息

分析物详细信息不可用

1
alpha-Hydroxyalprazolam
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2
Oxazepam-d5
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3
Oxazepam
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4
Alprazolam-d5
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5
Alprazolam
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6
Nordiazepam-d5
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7
Nordiazepam
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8
Lorazepam-d4
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9
Lorazepam
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10
Clonazepam-d4
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11
Clonazepam
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12
Temazepam-d5
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13
Temazepam
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14
Diazepam-d5
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15
Diazepam
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