Region

应用

Barbiturates in urine using Strata-X-Drug N and Kinetex C18 2.6µm 100x2.1mm

样品制备详细信息

Part Number :8B-S129-ECH
Description :Strata-X-Drug N 100u Polymer RP, 100mg/6mL, 30/Pk
Load :Load Sample
Wash 1 : 2 mLs of 0.1N HCl
Wash 2 : 2 mLs of Methanol/0.1N HCl (30:70)
Dry :10 min under full vacuum
Elution 1 : 2 mLs of Ethylacetate/IPA (85:15) (v:v)
Evaporate: :Evaporate to dryness
Reconstitute :1 mL 10% acetonitrile
Notes :Evaporate eluant to dryness under stream of N2 (50ºC). Reconstitute samples with 1mL of 10% acetonitrile

应用详细信息 (应用ID: 19724)

货号:00D-4462-AN
尺寸:100 x 2.1 mm ID
洗脱类型:Gradient
洗脱A:5mM Ammonium acetate
洗脱B:Acetonitrile
梯度程序:
步骤序号 时间 (分) 图片A 图片B
2 0 90 10
3 10 55 45
4 10.01 10 90
5 12 10 90
6 12.01 90 10
7 16 90 10

流速 (毫升/分钟):400 µL/min
冷却温度: 室温
检测: Mass Spectrometer (MS) @ amu (22°C)
检测器信息: SCIEX API 5000™
备注:SecurityGuard™ ULTRA Guard Cartridge System extends column lifetime.
- SecurityGuard ULTRA Cartridges, UHPLC C18 for 2.1mm ID Columns, 3/Pk Part No.: AJ0-8782
- Holder Part No.: AJ0-9000

分析物详细信息

分析物详细信息不可用

1
Phenobarbital-d5
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2
Phenobarbital
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3
Butalbital-d5

4
Butalbital
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5
Pentobarbital
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6
Amobarbital
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7
Secobarbital
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