Region

应用

Quantification of Carbamates Fungicides in Beverage by LC/MS/MS

样品制备详细信息

Part Number :8B-S100-TBJ
Description :Strata-X 33 µm Polymeric Reversed Phase, 30 mg / 3 mL, Tubes, 50/Pk
Condition 1 :1 mL Methanol
Condition 2 :1 mL 25 mM Ammonium acetete pH 5.5
Load :Load 1.40 mL Sample diluted in pretreated sample
Wash 1 :1 mL 25 mM Ammonium acetete pH 5.5
Wash 2 :1 mL Methanol/Water (15:85)
Dry :2 min at 10mm Hg
Elution 1 :0.5 mL 5% Formic acid in Methanol
Evaporate: :Evaporate to dryness
Reconstitute :1 mL Initial mobile phase

应用详细信息 (应用ID: 20025)

货号:00B-4439-B0
尺寸:50 x 2 mm ID
洗脱类型:Gradient
洗脱A:5mM ammonium formate
洗脱B:5mM ammonium formate in acetonitrile
梯度程序:
步骤序号 时间 (分) 图片A 图片B
1 0 85 15
2 2.5 5 95
3 4 5 95
4 4.01 85 15
5 8 85 15

流速 (毫升/分钟):0.5 mL/min
冷却温度: 28 °C
检测: Tandem Mass Spec (MS-MS) @ (22°C)
检测器信息: 3200 QTRAP
备注:SecurityGuard™ Guard Cartridge System extends column lifetime.
- SecurityGuard Cartridges, Gemini C18 4 x 2.0mm ID, 10/Pk Part No.: AJ0-7596
- Holder Part No.: KJ0-4282

分析物详细信息

分析物详细信息不可用

1
Aldicarb-sulfone
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2
Methomyl
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3
3-Hydroxycarbofuran
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4
Oxamyl
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5
Aldicarb
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6
Carbofuran
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7
Carbofuran-d3
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8
Methiocarb
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