Region

应用

Penicillins in Meat by LC/MS/MS

样品制备详细信息

Part Number :8B-S001-FBJ
Description :Strata C18-E (55 µm, 70 Å), 200 mg / 3 mL, Tubes, 50/Pk
Condition 1 :4 mL Methanol at 30 µL/min
Condition 2 :4 mL Water at 30 µL/min
Load :Load 2.00 mL Sample diluted in Filtrate
Wash 1 :4 mL 0.1% Formic Acid in water
Elution 1 :2 mL Acetonitrile at 30 µL/min
Elution 2 :2 mL Acetonitrile at 30 µL/min
Evaporate: :Evaporate to dryness
Reconstitute :200 µL Water
Notes :The equilibration time at conditon 0 was 4 minutes before each injection.

应用详细信息 (应用ID: 20028)

货号:00F-4439-E0
尺寸:150 x 4.6 mm ID
洗脱类型:Gradient
洗脱A:0.1% Ammonia in water
洗脱B:95% Acetronitrile, 5% water and 0.1% ammonia
梯度程序:
步骤序号 时间 (分) 图片A 图片B
1 0 98 2
2 2 98 2
3 2.42 90 10
4 6 50 50
5 6.1 0 100
6 6.6 0 100
7 6.8 98 2
8 8 98 2

流速 (毫升/分钟):0.8 mL/min
冷却温度: 40 °C
检测: Tandem Mass Spec (MS-MS) @ -4500 V (600°C)
检测器信息: 3200 QTRAP
备注:This separation uses IMethod Kit Part Number KH0-9047

SecurityGuard™ Guard Cartridge System extends column lifetime.
- SecurityGuard Cartridges, Gemini C18 4 x 3.0mm ID, 10/Pk Part No.: AJ0-7597
- Holder Part No.: KJ0-4282

分析物详细信息

分析物详细信息不可用

1
Amoxicillin
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2
Ampicillin
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3
Penicillin G
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4
Penicillin V
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5
Oxacillin
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6
Cloxacillin
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7
Nafcillin
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8
Dicloxacillin
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