Region

应用

Extraction and Analysis of Metronidazole in Facial Cleansers

样品制备详细信息

Part Number :8B-S029-TBJ
Description :Strata-X-C 33 µm Polymeric Strong Cation, 30 mg / 3 mL, Tubes, 50/Pk
Condition 1 : 1 mL of MeOH
Condition 2 : 1 mL of 0.1N HCl
Load :Load Sample
Wash 1 : 3 mL of 0.1N HCl
Wash 2 : 3 mL of MeOH
Wash 3 : 6 mL of Ethyl Acetate
Dry :5 min under full vacuum
Elution 1 : 1 mL of 5:95 NH4OH:MeOH (v:v)
Evaporate: :Evaporate to dryness
Reconstitute :200 µL 10:90 MeOH:0.1% Formic Acid
Notes :Evaporate to dryness at 50 C. Reconstitute in 200 uL of 10:90 MeOH:0.1% Formic Acid

应用详细信息 (应用ID: 20631)

货号:00B-4496-AN
尺寸:50 x 2.1 mm ID
洗脱类型:Gradient
洗脱A:0.1% Formic Acid
洗脱B:MeOH
梯度程序:
步骤序号 时间 (分) 图片A 图片B
1 0 95 5
2 2 60 40
3 3 60 40
4 3.1 95 5
5 5 95 5

流速 (毫升/分钟):300 µL/min
冷却温度: 25 °C
检测: Mass Spectrometer (MS) @ amu (650°C)
检测器信息: SCIEX API 4000™
备注:SecurityGuard™ ULTRA Guard Cartridge System extends column lifetime.
- SecurityGuard ULTRA Cartridges, UHPLC C18 for 2.1mm ID Columns, 3/Pk Part No.: AJ0-8782
- Holder Part No.: AJ0-9000

分析物详细信息

分析物详细信息不可用

1
Metronidazole
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2
13-C2 15-N-Metronidazole
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