Region

应用

Biogenic Amines by LCMS using Kinetex 1.7u C18 50x3.0mm

样品制备详细信息

Part Number :8B-S029-UBJ
Description :Strata-X-C 33 µm Polymeric Strong Cation, 60 mg / 3 mL, Tubes, 50/Pk
Condition 1 :3 mL Methanol at 1 mL/min
Condition 2 :4 mL Water
Load :Load Sample
Wash 1 :3 mL 0.1M HCl
Wash 2 :3 mL Methanol
Elution 1 :3 mL 0.2M Ammonia Solution made up in methanol
Evaporate: :Evaporate to dryness
Reconstitute :0 µL Mobile phase

应用详细信息 (应用ID: 20685)

货号:00B-4475-Y0
尺寸:50 x 3 mm ID
洗脱类型:Gradient
洗脱A:30mM Ammonium formate
洗脱B:Acetonitrile
梯度程序:
步骤序号 时间 (分) 图片A 图片B
1 0 80 20
2 3 40 60
3 3.1 0 100
4 4 0 100
5 4.1 80 20
6 5 80 20

流速 (毫升/分钟):600 µL/min
冷却温度: 室温
检测: Tandem Mass Spec (MS-MS) @ (22°C)
检测器信息: SCIEX API 4000™

分析物详细信息

分析物详细信息不可用

1
IQx
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2
8-MeIQx
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3
IQ
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4
7,8-DiMeIQx
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5
4,8-DiMeI-Qx
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6
MeIQ
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7
Trp-P-2
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8
Harman
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9
PhIP
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10
Norharman
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11
AaC
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12
MeAaC